• haohan2m*3mm工业乙酸甲酯测定10%聚己二酸乙二醇酯/401有机担体填充柱

    详细信息

     品牌:haohan  型号:2m*3mm  加工定制:是  
     测量范围:ppm  测量对象:乙酸甲酯  控温范围:200 ℃ 
     尺寸:2000 mm 重量:0.02 Kg 乙酸甲酯:10%聚己二酸乙二醇酯  
     401有机担体:非甲烷总烃  石墨化碳黑:零级空气发生器  氧化铝:*  
     硫化物:二甲二硫    
    乙酸甲酯是生产冰乙酸的副产品。乙酸甲酯中总酯含量约80%左右。根据色谱法定性的结果,浩瀚色谱(山东)应用技术开发有限公司进行了气相色谱分析的试验,以确定乙酸甲酯的含量。试验情况如下。 GC-790型气相色谱仪(热导检测器) 固定相:10%聚己二酸乙二醇酯/401有机担体填充柱 :长2m、内径4mm的不锈钢管汽化室温度:150℃检测室温度:140℃柱温:130℃桥流:200mA 氢载气流速:75mL/min 进样量:2μL 2.定性方法利用保留时间,用已知物直接对照进行定性。对乙酸甲酯样品的定性结果如图。

     

    名称:填充柱
    固定液·:10%聚己二酸乙二醇酯

    担体:401有机担体(0.25mm-0.18mm)/60-80目

    配比:载体:固定液=100:10
    型号:10%PEA/401
    应用:工业乙酸甲酯测定


    Methyl acetate is a by-product of the production of glacial acetic acid. The total ester content in methyl acetate is about 80%. According to the qualitative results of chromatography, Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. conducted a gas chromatography analysis test to determine the content of methyl acetate. The test situation is as follows. GC-790 gas chromatograph (thermal conductivity detector) Stationary phase: 10% polyethylene adipate/401 organic support packed column: stainless steel tube with a length of 2m and an inner diameter of 4mm Vaporization chamber temperature: 150℃ Detection chamber temperature : 140℃Column temperature: 130℃Bridge flow: 200mA Hydrogen carrier gas flow rate: 75mL/min Injection volume: 2μL 2. Qualitative method Use retention time to directly compare with known substances for qualitative determination. The qualitative results for the methyl acetate sample are shown in the figure.

    ​​​​​​​
    Name: Packed Column
    Fixative: 10% polyethylene adipate

    Carrier: 401 organic carrier (0.25mm-0.18mm)/60-80 mesh

    Ratio: Carrier: Fixative = 100:10
    Model: 10%PEA/401
    Application: Determination of Industrial Methyl Acetate

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