haohan氧化铝毛细管色谱柱应用之液化气分离HH-pLOT-AL2O3/Na2SO4

浩瀚色谱（山东）应用技术开发有限公司考察了多种Al2O3对低碳烃的保留性能,采用γ-Al2O3作固定相,2%Na2SO4水溶液脱活成功研制出0.32 mm×50 m Al2O3PLOT(porous layer open tubular)石英毛细管色谱柱。该柱对C1~C8低碳烃具有较强的分离能力,具有良好的选择性、柱惰性和较高的柱容量。建立了液化气的色谱分析方法,色谱条件:汽化160℃,检测180℃,柱温80℃,保持4 min,升速8℃/min,终温160℃,保持11 min;FID检测;载气(N2)柱前压0.042 MPa,分流比约180∶1,尾吹25mL/min,空气流量350 mL/min,氢气流量35 mL/min;进样量50μL。

名称：毛细管柱
型号：HH-pLOT-AL2O3/Na2SO4    
规格：50m*0.32mm*8um      
固定相：三氧化二铝
ZUI高使用温度：200°C

分离：液化气，天然气，煤气，费托合成气中轻烃C1-C8

Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. investigated the retention performance of various Al2O3 for low-carbon hydrocarbons. Using γ - Al2O3 as the stationary phase and 2% Na2SO4 aqueous solution for deactivation, a 0.32 mm × 50 m Al2O3PLOT (porous layer open tubular) quartz capillary chromatography column was successfully developed. This column has strong separation ability for C1~C8 low-carbon hydrocarbons, with good selectivity, column inertness, and high column capacity. A chromatographic analysis method for liquefied gas has been established, with chromatographic conditions: vaporization at 160 ℃, detection at 180 ℃, column temperature at 80 ℃, holding for 4 minutes, raising by 8 ℃/min, final temperature at 160 ℃, holding for 11 minutes; FID detection; The front pressure of the carrier gas (N2) column is 0.042 MPa, the split ratio is about 180:1, the tail blowing is 25 mL/min, the air flow rate is 350 mL/min, and the hydrogen flow rate is 35 mL/min; The injection volume is 50 μ L.
Name: Capillary Column
Model: HH-pLOT-AL2O3/Na2SO4
Specification: 50m * 0.32mm * 8um
Fixed phase: Aluminum oxide
ZUI high operating temperature: 200 ° C
Separation: Light hydrocarbons C1 to C8 in liquefied gas, natural gas, coal gas, and Fischer Tropsch synthesis gas