• haohan工业氨水测定专用HH-NH2-III填充柱应用赛默飞2m*1/8

    详细信息

     品牌:haohan  型号:2m*1/8  加工定制:是  
     规格:2m*3mm  长度:2000  内径:2.1  
     膜厚:1.0  工业氨水:HH-NH2-III  非甲烷总烃:氧化亚氮  
     二氧化碳:固定污染源废气  苯系物:分子筛  3%Dexil-300/Chromosorb W AW D:三甲胺  
    工业氨水的气相色谱测定是一个可行的方案,但需要特别注意氨的特性(强极性、易挥发、易吸附、易溶于水)以及工业氨水可能含有的杂质。

    核心挑战

    1. 强极性 & 易吸附: 氨分子极性极强,容易在进样口、色谱柱(尤其是非极性/弱极性柱)和检测器管路中发生吸附,导致峰拖尾、灵敏度下降、重现性差。

    2. 水含量高: 工业氨水通常含大量水(浓度在20%-30%左右)。水会严重干扰色谱分析,损坏色谱柱(特别是硅基固定相),在TCD上产生巨大响应,在FID上不响应但会导致基线不稳。

    3. 易挥发: 氨沸点低(-33°C),极易挥发,样品处理和进样需要快速、密封性好。

       

      浩瀚色谱(山东)应用技术开发有限公司,研制生产的《工业氨水测定专用填充色谱柱应用安捷伦 》,柱效高,分离好,在安捷伦,岛津,赛默飞,瓦里安,布鲁克,PE上结果满意。


      名称:氨水填充柱
      型号:HH-NH3-II
      规格:2m*1/8,60-80目

      zui高使用温度:200°C

       

      适用于:

      安捷伦490在线/便携,4890,5890,6890,7820,7890,8860,8890

      岛津GC-14C,GC-2010,GC-2014,GC-2030

      赛默飞1310,1300,1610,1600

      瓦里安3800系列

      布鲁克PE580,590,680,690

      磐诺A90,福立GC9790,华爱,天瑞,天美,GC7900,川仪,北分瑞利,东西电子,鲁南瑞虹,捷岛/科晓



     
    The gas chromatography determination of industrial ammonia water is a feasible solution, but special attention needs to be paid to the characteristics of ammonia (strong polarity, volatility, adsorption, solubility in water) and the impurities that industrial ammonia water may contain.
    Core Challenge
    Strong polarity&easy adsorption: Ammonia molecules have extremely strong polarity and are prone to adsorption in the injection port, chromatographic column (especially non-polar/weak polarity columns), and detector tubing, resulting in peak tailing, decreased sensitivity, and poor reproducibility.
    High water content: Industrial ammonia water usually contains a large amount of water (concentration around 20% -30%). Water can seriously interfere with chromatographic analysis, damage chromatographic columns (especially silicon-based stationary phases), produce significant response on TCD, and not respond on FID but can lead to unstable baseline.
    Volatile: Ammonia has a low boiling point (-33 ° C) and is highly volatile. Sample processing and injection require fast and well sealed conditions.
    Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. has developed and produced the "Agilent Application of Industrial Ammonia Determination Special Filled Chromatography Column", which has high column efficiency and good separation. The results are satisfactory on Agilent, Shimadzu, Thermo Fisher, Varian, Brooke, and PE.
    Name: Ammonia filled column
    Model: HH-NH3-II
    Specification: 2m * 1/8, 60-80 mesh
    Maximum operating temperature: 200 ° C
    Suitable for:
    Agilent 490 online/portable, 48905890689088608890
    Shimadzu GC-14C, GC-2010, GC-2014, GC-2030
    Thermo Fisher Scientific 1310130016101600
    Varian 3800 Series
    Brooke PE580590680690
    Panno A90, Fuli GC9790, Huaai, Tianrui, Tianmei, GC7900, Chuanyi, Beifen Ruili, Dongxi Electronics, Lunan Ruihong, Jiedao/Kexiao
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