haohan固定污染源排气中丙烯醛的测定岛津GC2014硬质玻璃柱gdx-502

1. 色谱分析条件：

   色谱柱：GDX-502 (60-80目，3m × 4mm)
2. 柱箱温度：140℃
3. 检测器温度：160℃ (FID)
4. 汽化室温度：160℃
5. 气体流速：载气 (N₂) 60 mL/min；燃气 (H₂) 50 mL/min；助燃气 (Air) 500 mL/min

6. 校准与定量：

7. 通常用外标法绘制校准曲线（例如0-100 mg/m³范围内至少5个浓度点）。
8. 取1mL气体样品（或5mL5）注入色谱仪。样品浓度过高可用纯净空气或氮气稀释5。

9. 结果计算：

10. 通过校准曲线查得或回归方程计算样品中丙烯醛的浓度。
11. 根据采气体积、温度、压力等换算为标准状态下的浓度。

浩瀚色谱（山东）应用技术开发有限公司，采用固定污染源中丙xi醛的测定GDX502玻璃色谱柱测定固定污染源排气中丙xi醛，面积外标法定量，在安捷伦，岛津，赛默飞，瓦里安，布鲁克，PE上安装使用，效果良好。

名称：硬质玻璃柱

规格：3m*4mm

型号：GDX-502，60/80目

应用：HJ/T 36-1999 固定污染源排气中丙xi醛的测定 气相色谱法

适用于：

安捷伦490在线/便携，4890,5890,6890,7820,7890,8860,8890

岛津GC-14C，GC-2010，GC-2014，GC-2030

赛默飞1310,1300,1610,1600

瓦里安3800系列

布鲁克PE580,590,680,690

磐诺A90，福立GC9790，华爱，天瑞，天美，GC7900，川仪，北分瑞利，东西电子，鲁南瑞虹，捷岛/科晓

Instability of Acrolein: Acrolein is very prone to oxidation, so after sampling, it should be strictly protected from light, stored at low temperatures, and analyzed as soon as possible to reduce losses and ensure accurate results
This standard is applicable to the determination of acrolein in organized and unorganized emissions from fixed pollution sources. The detection limit of this standard is 0.1mg/m3. When the injection volume is 1ml, the concentration range for quantitative determination is 0.31-1.0 × 102mg/m3.
The GDX-502 packed column gas chromatography method specified in the HJ/T 36-1999 standard is a classic method for determining acrolein in exhaust gas from fixed pollution sources. The detection limit, quantitative range, precision, and accuracy of the method can meet the requirements of current environmental monitoring
Chromatographic analysis conditions:
Chromatography column: GDX-502 (60-80 mesh, 3m × 4mm)
Column box temperature: 140 ℃
Detector temperature: 160 ℃ (FID)
Vaporization chamber temperature: 160 ℃
Gas flow rate: carrier gas (N ₂) 60 mL/min; Gas (H ₂) 50 mL/min; Gas (Air) 500 mL/min
Calibration and Quantification:
Usually, the calibration curve is drawn using the external standard method (for example, at least 5 concentration points within the range of 0-100 mg/m ³).
Take 1mL of gas sample (or 5mL) and inject it into the chromatograph. If the sample concentration is too high, pure air or nitrogen can be used to dilute 5.
Result calculation:
Calculate the concentration of acrolein in the sample through calibration curve or regression equation.
Convert to standard concentration based on gas production volume, temperature, pressure, etc.
Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. uses GDX502 glass chromatography column to determine formaldehyde in exhaust gas from fixed pollution sources, and uses area external standard method for quantification. It has been installed and used on Agilent, Shimadzu, Thermo Fisher, Varian, Brooke, and PE with good results.
Name: Hard Glass Column
Specification: 3m * 4mm
Model: GDX-502, 60/80 mesh
Application: HJ/T 36-1999 Determination of Propionaldehyde in Fixed Source Exhaust Gas by Gas Chromatography
Suitable for:
Agilent 490 online/portable, 48905890689088608890
Shimadzu GC-14C, GC-2010, GC-2014, GC-2030
Thermo Fisher Scientific 1310130016101600
Varian 3800 Series
Brooke PE580590680690
Panno A90, Fuli GC9790, Huaai, Tianrui, Tianmei, GC7900， Chuanyi, Beifen Ruili, Dongxi Electronics, Lunan Ruihong, Jiedao/Kexiao