| 加工定制:是 | | 品牌:翔鹰技术 | | 型号:XiangyingGC7990plus | |
| 测量范围:ppm | | 测量对象:过氧化双环己胺 | | 控温范围:400 ℃ | |
| 功率:2000 w | | 尺寸:480 mm | | 重量:46 kg | |
| 乙二醇:过氧化双环己胺 | | 芝麻香白酒:3-甲硫基丙醇 | | 液化气:二甲醚 | |
| 室内空气污染物:TVOC | | 植物油:6号溶剂残留 | | | |
1 1 'oxidation dicyclohexyl amine (1 1' PXA) is used in the production of nylon 12 raw materials, is a product of cyclohexanone, ammonia and hydrogen peroxide formation under certain conditions. The impurity production of cyclohexanone, ammonia and hydrogen peroxide also contains 11 'two hydroxy cyclohexyl peroxide. Since 11 'over dicyclohexyl amine oxide is very unstable, low melting point, can not use distillation method analysis
Tengzhou Xiangying Analysis Technology Co. Ltd. by XiangyingGC7990plus gas chromatography, determination of dicyclohexyl amine oxide,
The results showed that the cyclohexanone, 1 1 'too dicyclohexyl amine oxide determination results of the relative standard deviation was less than 1 5%, the recovery rate 96% ~ 100% and 99% ~ 10%, respectively. The method is simple, sensitive, accurate and reproducible.
1 1′ 过氧化双环己胺 (1 1′ PXA)是用来生产尼龙 12的原料 ,是环己酮、氨和双氧水在一定条件下生成的产物。环己酮、氨和双氧水的生成产物中还含有 1 1′ 二羟基二环己基过氧化物等杂质。由于 1 1′ 过氧化双环己胺极不稳定 ,熔点低 ,不可能用馏程分析法进
滕州市翔鹰分析技术有限公司采用XiangyingGC7990plus气相色谱仪,测定过氧化双环己胺,
结果表明 :环己酮、1 1′ 过氧化双环己胺测定结果的相对标准偏差均小于 1 5 %,回收率分别为 96 38%~ 10 0 8%和 99 31%~ 10 3 1%。方法简便、灵敏、准确、重现性好
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