• 催化合成2-乙基蒽醌的气相色谱分析

    详细信息

     加工定制:是  品牌:翔鹰技术  型号:XiangyingGC7990plus  
     测量范围:ppm  测量对象:2-乙基蒽醌的气相色谱分析  控温范围:400 ℃ 
     功率:2000 w 尺寸:480 mm 重量:46 kg 
     咔唑:2-乙基蒽醌的气相色谱分析  :蒽醌  煤焦油:粗苯  
     沥青:室内空气污染物  植物油:顶空进样器   

                     2-ethylanthraquinone (2-EAQ) is a light yellow powder or light yellow flaky solid is 2-alkyl anthraquinone dosage is the biggest and most important one of the species, mainly used for synthesis of hydrogen peroxide by anthraquinone load medium for hydrogen, can also be used for preparing photosensitive compound, optical screen photosensitive resin, polymerization catalyst and dyestuff intermediates etc.. At present, 2-EAQ is widely used in industrial production of phthalic anhydride method, mainly divided into two steps: o
                       In Tengzhou City Xiangying Analysis Technology Co., Ltd. phthalic anhydride and ethylbenzene one-step synthesis of 2 - ethyl - anthraquinone XiangyingGC7990plus gas chromatographic analysis method was established. The 2- * 0.25mm * 0.25 m and the hydrogen flame ionization detector were selected as the internal standard. The standard curve method was used to carry out the quantitative analysis of the reaction solution in the reaction solution with the method of the internal standard curve method. Experimental results show that the analysis method in the experimental concentration range, the linear relationship is good, linear correlation coefficient of phthalic anhydride, 2-ethyl anthraquinone were 0.998 32 and 0.999 72 and recovery rate were to 101.94% 98.80% ~ 102.67% and 98.37% relative standard deviation respectively 0.87% ~ 2.08% and 0.67% to 1.76%. The method is simple, rapid, high accuracy and good reproducibility.
                2-乙基蒽醌(2-EAQ)为浅黄色粉末或亮黄色鳞片状固体,是2-烷基蒽醌中用量***大也是***重要的品种之一,主要用作蒽醌法合成过氧化氢的载氢介质,也可以用作制备感光化合物、光筛树脂、光敏聚合催化剂和染料中间体等。目前,2-EAQ的工业化生产普遍采用苯酐法,主要分为两步:邻
       
     滕州市翔鹰分析技术有限公司建立了邻苯二甲酸酐和乙苯一步法合成2-乙基蒽醌的XiangyingGC7990plus气相色谱分析方法。选择毛细管柱(30m×0.25mm×0.25μm)和氢火焰离子化检测器,以萘为内标物,采用内标标准曲线法对反应液中的邻苯二甲酸酐和2-乙基蒽醌进行定量分析。实验结果表明,该分析方法在实验浓度范围内线性关系良好,对邻苯二甲酸酐、2-乙基蒽醌的线性相关系数分别为0.998 32和0.999 72,回收率分别为98.80%~102.67%和98.37%~101.94%,相对标准偏差分别为0.87%~2.08%和0.67%~1.76%。该方法具有简单、快速、准确度高、重现性好的特点。


    The Chinese technology, analysis technology leader
    The gas chromatography technology, the industry benchmark enterprise
    1 focused on the development of gas chromatograph
    2 committed to becoming a leading supplier of analytical instruments in China
    3 to provide you with the most powerful support
    4 super high cost quality products
    5 high quality and perfect after sales service
    翔鹰技术,中国分析技术的领跑者
    翔鹰技术,气相色谱行业*企业
    1.专注气相色谱仪的研制
    2.致力于成为国内分析仪器领先供应商
    3.为你提供***强有力的支持
    4.超高性价比品质过硬产品
    5.优质完善快捷的售后服务


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