• Shimadzu 玻璃球为填料的色谱柱应用岛津GC2014测定药典二氧化碳2015,,4mm×0.8m,80目

    详细信息

     品牌:Shimadzu  型号:4mm×0.8m,80目  加工定制:是  
     规格:4mm×0.8m,80目  长度:800  内径:3  
     膜厚:0.2  4mm×0.8m,80目:药典  2015:玻璃球  
     二氧化碳:碳氢化合物  净化装置:甲烷  3%Dexil-300/Chromosorb W AW D:糖苷  
    碳氢化合物 取本品作为供试品气体,取甲烷含量为0.0020%的气体(以氮气为稀释剂)作为对照气体,照气相色谱法(通则0521)试验,用玻璃球为填料的色谱柱(4mm×0.8m,80目);柱温为110℃;进样口温度为110℃;检测器为火焰离子化检测器,温度为120℃。量取供试品气体与对照气体,注入色谱仪,在净化温度为360℃时测得的峰面积为相应空白值;量取供试品气体与对照气体,注入色谱仪,测定峰面积,减去相应空白值后的峰面积为校正峰面积。按外标法以校正峰面积计算,含碳氢化合物(以甲烷计)不得过0.0020%。

    浩瀚色谱研制的玻璃球色谱柱,柱效高,分离好,和岛津,赛默飞,瓦里安,布鲁克,pe,磐诺,福立,北分瑞利等仪器,能实现互联互通,结果满意。

    名称:色谱柱
    固定相:玻璃球
    粒度:80mesh
    规格:0.8m*4mm
    型号:HH-BLQ
    应用:2015/2020年版药典二氧化碳中碳氢化合物的分析
     

    Hydrocarbons: This product is used as the test gas, and a gas with a methane content of 0.0020% (diluted with nitrogen) is used as the control gas. The gas chromatography method (General Rule 0521) is used for testing, and a chromatography column (4mm × 0.8m, 80 mesh) filled with glass spheres is used; The column temperature is 110 ℃; The inlet temperature is 110 ℃; The detector is a flame ionization detector with a temperature of 120 ℃. Measure the test gas and control gas, inject them into the chromatograph, and measure the peak area at a purification temperature of 360 ℃ as the corresponding blank value; Measure the test gas and control gas, inject them into the chromatograph, measure the peak area, and subtract the corresponding blank value to obtain the corrected peak area. According to the external standard method, the corrected peak area should not exceed 0.0020% for hydrocarbons (calculated as methane).
    The glass sphere chromatography column developed by Haohan Chromatography has high column efficiency and good separation. It can be interconnected with instruments such as Shimadzu, Thermo Fisher Scientific, Varian, Brooke, PE, Panno, Fuli, and Beifen Raleigh, and the results are satisfactory.
    Name: Chromatographic Column
    Fixed phase: glass ball
    Granularity: 80mesh
    Specification: 0.8m * 4mm
    Model: HH-BLQ
    Application: Analysis of Hydrocarbons in Carbon Dioxide in the 2015/2020 Pharmacopoeia
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