• 浩瀚2025年版药典二氧化碳分析玻璃球色谱柱应用安捷伦8890上0.8m*4mm

    详细信息

     品牌:浩瀚  型号:0.8m*4mm  加工定制:是  
     规格:0.8m*4mm  长度:800  内径:3  
     膜厚:20  2025年版:药典  二氧化碳:碳氢化合物  
     CO2:甲烷  标气:玻璃球  色谱柱:净化装置  
    二氧化碳中碳氢化合物(以甲烷计)的含量限度为不得超过0.0020%(体积比)。分析时需采用气相色谱法(通则0521),并使用以下规格的色谱柱
     

    名称:玻璃球填充柱

    规格:0.8m*4mm,80目

    zui高使用温度:300°C

    应用:2025年版药典二氧化碳中碳氢化合物的测定
     

    核心的色谱分析条件和仪器配置如下表所示:

    项目 具体条件/说明
    色谱柱 玻璃球填充柱,规格 0.8m × 4mm,80目
    温度设置 柱温:110℃;进样口温度:110℃;检测器温度:250℃。
    检测器 氢火焰离子化检测器(FID)。
    定量方法 外标法。使用甲烷含量为0.0020%的对照气体,以校正峰面积计算。
    关键步骤 需在净化温度360℃下测定供试品和对照气体的空白值,并从实测峰面积中扣除。
    仪器适配 色谱柱的接口规格(如1/8英寸)需与您使用的气相色谱仪品牌和型号匹配(如安捷伦、珀金埃尔默等)。

    浩瀚色谱(山东)应用技术开发有限公司,研制《药典二氧化碳玻璃球色谱柱应用岛津2014》,在安捷伦,岛津,赛默飞,PE,布鲁克,瓦里安等仪器安装使用,面积外标法定量,结果满意。
     

    适用于:

    安捷伦490在线/便携,4890,5890,6890,7820,7890,8860,8890

    岛津GC-14C,GC-2010,GC-2014,GC-2030

    赛默飞1310,1300,1610,1600

    瓦里安3800系列

    布鲁克PE580,590,680,690

    磐诺A90,福立GC9790,华爱,天瑞,天美,GC7900,川仪,北分瑞利,东西电子,鲁南瑞虹,捷岛/科晓
     

    The limit for the content of hydrocarbons (calculated as methane) in carbon dioxide shall not exceed 0.0020% by volume. Gas chromatography (General Rule 0521) should be used for analysis, and the following specifications of chromatographic columns should be used
    Name: Glass Ball Filled Column
    Specification: 0.8m * 4mm, 80 mesh
    Maximum operating temperature: 300 ° C
    Application: Determination of Hydrocarbons in Carbon Dioxide in the 2025 Pharmacopoeia
    The core chromatographic analysis conditions and instrument configuration are shown in the following table:
    Specific project conditions/description
    Chromatographic column filled with glass spheres, specification 0.8m × 4mm, 80 mesh.
    Temperature setting column temperature: 110 ℃; Injection port temperature: 110 ℃; Detector temperature: 250 ℃.
    Detector: Hydrogen Flame Ionization Detector (FID).
    Quantitative method external standard method. Use a control gas with a methane content of 0.0020% to calibrate the peak area calculation.
    The key step is to measure the blank values of the test sample and control gas at a purification temperature of 360 ℃, and deduct them from the measured peak area.
    The interface specifications of the instrument adapted chromatography column (such as 1/8 inch) need to match the brand and model of the gas chromatograph you are using (such as Agilent, PerkinElmer, etc.).
    Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. has developed the "Pharmacopoeia CO2 Glass Ball Chromatography Column Application Shimadzu 2014", which has been used in Agilent, Shimadzu, and Thermo Fisher Scientific, PE, Brooke, Varian and other instruments were installed and used, and the area external standard method was used for quantification, with satisfactory results.
    Suitable for:
    Agilent 490 online/portable, 48905890689088608890
    Shimadzu GC-14C, GC-2010, GC-2014, GC-2030
    Thermo Fisher Scientific 1310130016101600
    Varian 3800 Series
    Brooke PE580590680690
    Panno A90, Fuli GC9790, Huaai, Tianrui, Tianmei, GC7900, Chuanyi, Beifen Ruili, Dongxi Electronics, Lunan Ruihong, Jiedao/Kexiao

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