• 浩瀚氯乙酰氯直接进样分析专用毛细管柱HHLYS3698-30

    详细信息

     品牌:浩瀚  型号:HHLYS3698-30  加工定制:是  
     测量范围:ppm  测量对象:氯乙酰氯  控温范围:250 ℃ 
     尺寸:30000 mm 重量:0.02 Kg 氯乙酰氯:二氯乙酰氯  
     三氯乙酰氯:氯乙酸  热解吸仪:裂解进样器  增塑剂:塑化剂  
     氨气:氨气    
    氯乙酰氯作为酰化剂广泛用于药物和农药的合成。酰氯的分析方法之一是以氨或胺与酰氯反应生成酰胺和酸,从而测得酰氯的含量(Ind Eng Chem,Anal ed 1946,18:444)。另有以醇与酰氯反应生成酯和酸的分析方法(Analyst 1953,78:675)较前法为优,但作者发现,该法有较大误差。原因是氯乙酰氯和醇酯化时反应激烈,部分氯化氢与氯乙酰氯易于逸出,致使分析结果偏低。

    浩瀚色谱(山东)应用技术开发有限公司研发专用毛细管柱用气相色谱法分析氯乙酰氯,结果表明,此法分离效果好,准确度高,可用于氯乙酰氯工业生产的中间控制和产品质量分析。

    此柱直接进样测定氯乙酰氯,二氯乙酰氯,三氯乙酰氯,氯乙酸和氯乙酸酐等杂质,效果良好。
     

    名称:毛细管柱

    规格:30m*0.32mm*0.5um

    型号:HHLYS3698-30

    应用:工业氯乙酰氯测定



    Chloroacetyl chloride is widely used as an acylating agent in the synthesis of drugs and pesticides. One of the analysis methods of acid chloride is to react ammonia or amine with acid chloride to generate amide and acid, thereby measuring the content of acid chloride (Ind Eng Chem, Anal ed 1946, 18:444). In addition, the analysis method (Analyst 1953, 78: 675) that uses alcohol and acid chloride to react to produce esters and acids is better than the previous method, but the author found that this method has larger errors. The reason is that the reaction of chloroacetyl chloride and alcohol is fierce during esterification, and part of hydrogen chloride and chloroacetyl chloride are easy to escape, resulting in low analysis results.

    Haohan Chromatography (Shandong) Applied Technology Development Co., Ltd. has developed a special capillary column to analyze chloroacetyl chloride by gas chromatography. The results show that this method has good separation effect and high accuracy, and can be used for intermediate control of chloroacetyl chloride industrial production and product quality analysis. .

    The column is directly injected to determine impurities such as chloroacetyl chloride, dichloroacetyl chloride, trichloroacetyl chloride, chloroacetic acid and chloroacetic anhydride, with good results.

    Name: Capillary Column

    Specification: 30m*0.32mm*0.5um

    Model: HHLYS3698-30

    Application: Determination of industrial chloroacetyl chloride 

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